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KCI 후보
Monovalent와 bivalent aminoantipyrine 유도체의 합성과 항염 진통활성
Synthesis and Antiinflammatory-analgesic Activity of Monovalent and Bivalent Aminoantipyrines
김승재, 권오혁, 전상철, 박상민, 임채욱, 임철부
약학회지 46권 3호 149-154(6pages)

Six novel 4-aminoantipyrine derivatives as potential nonsteroidal antiinflammatory and analgesic compounds were prepared and their antiinflammatory-analgesic activity were compared with antiprine. Succinyl chloride and Ac $_2$O were reacted with glycine, respectively, to give glycine compounds (3-4, 9-10), which were treated with hydroxysuccinimide and dicyclohexyl carbodiimide to yield active esters (5-6, 11-12), and then reacted with 4-aminoantipyrine to prepare 4-aminoantipyrine derivatives (7-8, 13-14). 4-Aminoantipyrine reacted with succinyl chloride and Ac $_2$O, respectively, to give succinyl bis aminoantipyrine (15) and acetyl aminoantipyrine (16). Compounds (7), (8) and (13) gave comparable antiinflammatory activity to antipyrine.

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