3- ( 3- Amino -1- Phenylethyl )-2- Methylindole 합성

이성환

한국응용생명화학회 한국응용생명화학회지 3- ( 3- Amino -1- Phenylethyl )-2- Methylindole 합성

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Synthesis of 3- ( 2- Amino -1- phenylethyl ) -2- methylindole 1. Synthesis of 3 - ( 2 - Nitro -1- phenylethyl -2- methylindole )

이성환 ( Sung Whan Lee )

한국응용생명화학회 1960.06

한국응용생명화학회지 vol. 1 43-47(5pages)

UCI I410-ECN-0102-2008-520-000750340

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Abstract

1). By means of the F.H. Allene and James Allenes method of the α-methylindole synthesis, 2-methylindole was prepared with the Acetyl-o-toluidine and NaNH₂. yield; 88% mp. 56.5∼57℃. 2). 23.7 gr of 3-(-Nitro-l-phenylethyl)-2-melthylindole was prepared with 0.1 ㏖. of the 2-methylindole and 0.1 ㏖. of the β-Nitrostyrene. yield : 84.6%, mp. 104∼105℃. 3). Analytical results. Calcd. fur C_(17)H_(16)N₂O₂: C, 72.84; H, 5.63; N, 9.99. Found: C, 72.62; H, 5.63; N, 9.79.

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