18.97.14.81
18.97.14.81
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병풀 (Centella asiatica) 엑스 - 베타시클로덱스트린 고체 분산체를 함유한 폴록사머 407 히드로겔 제조 및 피부투과
Preparation and Skin Permeation of Poloxamer 407 Hydrogel with Extract of Cantella asiatica-β-Cyclodextrin Solid Dispersion System
김경국 , 곽은선 , 이계원 , 박진규 , 박목순 , 지웅길 ( Kyoung Kook Kim , Eun Sun Kwak , Gye Won Lee , Jin Kyu Park , Mork Soon Park , Ung Kil Jee )
UCI I410-ECN-0102-2008-510-000811491

Extract of Centella asiatica(ECA), which is poorly water-soluble extract from the Centella asiatica is known to express excellent wound healing properties. ECA-β-cyclodextrin (asiaticoside-β-cyclodextrin and genin-β-cyclodextrin) solid dispersion system, which was prepared by freeze-drying method, was formulated as gels containing poloxamer 407 and propylene glycol, and evaluated with respect to their viscosity, stability, skin permeation and drug amount in the skin of hairless mouse. The average molar ratio asiaticoside-β-CD and genin-β-CD was 1:1.7 and 1:22. respectively. When the molar ratio of genin and β-CD was 1:5, madecassic acid made 100% solid dispersion system and asiatic acid about 65%. In dissolution study. >99% of asiaticoside from asiaticoside-β-CD was dissolved in 5 minutes, and >99% madecassic acid and >64% asiatic acid from genin-β-CD. The apparent viscosity of poloxamer 407 gels with ECA-β-CD solid dispersion system increased in proportion to poloxamer 407 and propylene glycol concentration. In the accelerated stability test, all ECA-β-CD poloxamer 407 gels showed that asiaticoside was most stable and madecassic acid stable and asiatic acid similar to stability of gel with free ECA. The permeation amount of asiaticoside in poloxamer gels through hairless mouse skin decreased as the concentration of poloxamer 407 increased. When propylene glycol was added at the level of 10%, the permeation amount of asiaticoside at poloxamer gels through hairless mouse skin increased but from 15% it decreased. The permeation of asiaticoside into the skin of hairless mouse was estimated to be about 0.10㎍/㎠.

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