This survey was carried out to determine sulfamethazine residues in urine, kidney and muscle of slaughtered pigs. For this investigation, 20 samples for export and 30 samples for domestic market were collected at slaughterplant in Anyang city from the early of November to the end of December and comparatively were analyzed by SOS test kit and HPLC the results obtained were summarized as follows: 1. Five of 50 samples of swine urine which were inspected by SOS test kit were appeared to sulfamethazine positive. 2. The sulfamethazine residue in one of 50 samples of swine muscle was exceeded 0.lppm 3. The positive samples by SOS test kit were agreed with the results of HPLC quantitative analysis