공업용 TiO₂, K₂CO₃, K₂MoO₄를 출발원료로 사용하여 소성법과 융계법에 의해 육티탄산칼륨 섬유를 합성하였다. 소성법의 경우 비등수로 처리한 후의 여액이 pH 9 이상의 알칼리성이 되므로 적절한 중화 처리가 필요하였으며, 칼륨 성분의 회수는 미량이므로 회수한다는 것이 경제적으로 부적합하였다. 또한 융제법의 경우 초생상 10g을 100ml로 10번 처리하였을 때 융제인 K₂MoO₄중 Mo성분이 96.1%, K성분이 91.8%가 회수되었다.

Potassium hexatitanate whisker was effectively prepared with calcination and flux method by using industrial TiO₂, K₂CO₃and K₂MoO₄ as the starting materials. When it was synthesized by the calcination method, the filtrate after boiling water treatment was required a neutralization, as the pH of filtrate was higher than 9. Because K component was very small, recovery of K component was not economically suitable. In case of flux method, flux was recovered 96.1% of Mo component and 91.8% of K component at K₂MoO₄ for 10th treatment in boiling water of 100ml to l0g.