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SCIE SCOPUS
Dual Affinity Tag 을 이용한 Human Hepatitis B Virus Polymerase 의 발현과 정제
Expression and Purification of Human Hepatitis B Virus Polymerase with a Dual Affinity Tag
곽동석 , 김자영 , 이영일 , 정구홍 ( Dong Seok Kwak , Ja Young Kim , Young Il Lee , Gu Hung Jung )
UCI I410-ECN-0102-2009-470-007056733

To improve human hepatitis B virus (HBV) polymerase expression in E. coli, we introduced His6 tag to the C-terminus of HBV polymerase. This expression vector, pMPH can direct expression of HBV polymerase with maltose binding protein (MBP) at its N-terminus and a His6 tag at its C-terminus. This allows for the purification of full-size HBV polymerase by a sequential two-step procedure on amylose resin and Ni2+-NTA resin. When MBP/PoI/His fusion protein was purified using amylose resin affinity chromatography, DNA-dependent DNA polymerase (DDDP) specific activity was 3.8 fold higher, and RNA-dependent DNA polymerase (RDDP) specific activity was 2.3 fold higher than those of MBP/PoI fusion protein. Based on these data, the fusion MBP/PoI protein with His6 tag increased the stability of polymerase and prevented its degradation. Since His6 tag is chelated Ni2+-NTA resin, amylose column-purified recombinant protein was reloaded on the second Ni2+-NTA column. The polymerase activity of this Ni2+-NTA column-purified MBP/PoI/His fusion protein was higher than that of amylose column purified MBP/PoI/His fusion protein or MPB/PoI fusion protein. The DDDP specific activity was 16.5 fold higher, and the RDDP specific activity was 5.0 fold higher than that of MBP/PoI fusion protein.

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