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18.97.14.89
18.97.14.89
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SCIE SCOPUS
E . coli 에 의해 생산된 재조합 사람 프리트롬빈 2 의 정제 및 활성화
Purification and Activation of Recombinant Human Prethrombin 2 Produced in E . coli
소인섭 , 이승철 , 김수원 , 함경수 , 김지영 ( In Seop So , Seung Cheol Lee , Soo Won Kim , Kyung Soo Hahm , Ji Young Kim )
BMB Reports vol. 25 iss. 1 60-65(6pages)
UCI I410-ECN-0102-2008-470-002208339

Human prethrombin 2 was purified from a recombinant E. coli cells in which human prethrombin 2 was produced as insoluble aggregates, amounting to 5 to 10% of the total bacterial proteins. Isolation of inclusion bodies and the subsequent solubilization of the insoluble proteins in a denaturing solution containing sodium dodecyl sulfate and dithiothreitol yielded good recovery of prethrombin 2 with at least 75% purity. Prethrombin 2 was further purified by two passages of Sephacryl S-200 gel chromatography. The purified prethrombin 2 was reacted with the polyclonal antibodies against human prothrombin. The N-terminal sequence of the prethrombin 2 was same as that of the native human prethrombin 2. The purified prethrombin 2 was renatured by stepwise removal of the denaturants by slow dialysis. The renatured prethrombin 2 was activated to thrombin by ecarin, a prothrombin activator from Echis carinatus and the thrombin activity generated was detected by a chromogenic assay. This study showed that recombinant prethrombin 2 produced in E. coli could be converted to thrombin.

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